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Nucleic Acids Symposium Series 1999 42(1):5-6; doi:10.1093/nass/42.1.5
© 1999 by Oxford University Press
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Synthesis and biological activity of unusual nucleosides having 3,4-bis(hydroxymethyl) thietane ring as a sugar moiety

Eiko Ichikawa1, Shosuke Yamamura1 and Kuniki Kato2

1 Department of Chemistry, Faculty of Science and Technology, Keio University, Hiyoshi, Yokohama 223, Japan, 2 Research Laboratories, Pharmaceuticals Group, Nippon Kayaku Co. Ltd. Shimo, Kita-ku, Tokyo 115, Japan

The enantiomerically pure synthesis of 9-[(2'S, 3'S)-bis(hydroxymethyl)thietan-1'-yl]adenine 2, 3'-thio analog of oxetanocin A, was achieved via coupling of silylated 6-chloropurine and sulfoxide 16 under Pummerer reaction conditions.


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